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Welcome to the HIGP Infrared Spectroscopy Lab. This laboratory supports
studies of the vibrational, or thermal infrared, properties of rocks
(including meteorites) and minerals, using both emission and reflection
measurement techniques. Our primary users are interested in understanding
the variation in spectral characteristics of samples of differing mineralogies,
chemistries, structures, particle sizes, shock levels, etc. The knowledge that
is gained from these studies is applied to the analysis of infrared spectra of
unknown samples, as well as remote sensing data collected over Earth and Mars.
The lab is equipped with a Nicolet 470 FTIR spectrometer with a CsI
beamsplitter for coverage to 200 cm-1. The spectrometer is
configured for both hemispherical reflectance and emission measurements.
The hemispherical reflectance attachment is provided by
Dr. Paul Lucey. The emission configuration is
modeled after the configuration at the
Thermal Emission Spectrometer (TES) laboratory at Arizona
State University. We welcome opportunities to collaborate on
projects with investigators from other institutions.
Watch this page for updates and information about the status of our lab.
14 March 2006
Although both the reflectance and emission capabilities have been available for about a year, we have not had our final calibration blackbodies for the emission side until recently. We are beginning our final reproducability characterization and expect to have results available in a month or two. The photos of the lab have been updated (see links below for 06 Nov. 2004)
.
17 March 2005
Download our
LPSC poster showing the instrument and initial data. (~2MB PDF file)
21 February 2005
Read about the laboratory setup in our 2005 Lunar and Planetary Science Conference abstract. In other news,
we have designed a sample stage for the emission side that will allow us to make
fine adjustments to sample position in the x and y directions in addition to selecting
the spot size via height adjustments. This stage will permit
analysis of much smaller samples than previously has been possible.
06 Novemberr 2004
New photos of the current lab configuration.
03 November 2004
Emission spectra of quartz
and a granite slab.
31 October 2004
Happy Halloween! The emission set up is assembled and collecting data.
Look for our first spectra to show up here in the next day or two. We are
still waiting for our blackbody calibration targets to be fabricated, but
for the moment, we are using IR-black sample cups as cal targets, and the
data quality is very impressive.
10 July 2004
The emission set up is coming along nicely; nearly all of the major parts
are in hand and ready for assembly. The last major pieces to come are the blackbody
calibration targets. Dr. Mike Ramsey at Univ. Pittsburgh is testing a new design
for the blackbodies, which are significantly smaller than the model in use at ASU
currently. The first of these has been built and is about to be tested for accuracy,
precision, and reproducibility at the Arizona State Univ. lab. Once these tests
are completed, and the new design finalized, three pairs will be manufactured and all
three institutions will have identical blackbody targets. Once these cal targets
are in hand at UH, we'll begin the
characterization of our emission setup and open for business!
6 February 2004
Since last year, we've moved the spectrometer to a new, more conveniently
located lab with lower humidity, and the purge gas generator is keeping the Nexus
scrubbed of CO2 and dry inside. We've made an improvement to the
hemispherical reflectance portion of the spectrometer. We replaced the external
MCT detector with one that provides a higher SNR at a lower number of scans. The
emission setup is moving ahead slowly but surely. It's likely to be several months
before it's ready for use, as several of the components must be custom manufactured.
30 January 2003
We collected our first data today, and they look great. The
Labsphere hemispherical reflectance
attachment covers the wavelength range from ~4000 - 600 cm-1 using
the spectrometer's internal CsI beamsplitter and an external liquid nitrogen-cooled
MCT detector.
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